Influence of Water Content on Thixotropic Strength Recovery of Zhanjiang Formation Structural Clay

XIE Yan-hua, TANG Bin, XU Ji-cheng, HAN Wei-chao, ZHANG Bing-hui

Journal of Changjiang River Scientific Research Institute ›› 2026, Vol. 43 ›› Issue (4) : 166-174.

PDF(9256 KB)
PDF(9256 KB)
Journal of Changjiang River Scientific Research Institute ›› 2026, Vol. 43 ›› Issue (4) : 166-174. DOI: 10.11988/ckyyb.20250292
ROCK-SOIL ENGINEERING

Influence of Water Content on Thixotropic Strength Recovery of Zhanjiang Formation Structural Clay

Author information +
History +

Abstract

[Objective] This study focuses on water content as the key controlling factor to clarify the time-dependent patterns of thixotropic strength recovery of Zhanjiang Formation structural clay under different initial water contents. The microscopic mechanism is interpreted through three pathways: pore structure evolution, particle reorganization, and water action. The findings are expected to provide experimental evidence and theoretical support for predicting strength recovery and evaluating the stability of thixotropic clay foundations. [Methods] Remolded Zhanjiang Formation structural clay specimens were prepared and subjected to a 150-day thixotropy test. Specimens at different thixotropic durations were investigated using macroscopic and microscopic tests. For macromechanical testing, unconfined compressive strength (UCS) tests were conducted on cylindrical specimens. Direct shear tests were conducted on ring-knife specimens to obtain UCS, cohesion (c), and internal friction angle (φ), which were used to evaluate thixotropic evolution. A thixotropic strength ratio was defined as At = mt/m0, and two indicators—At(q) (based on UCS) and At(τ) (based on cohesion)—were used to compare recovery characteristics among different strength parameters. For microstructure, fabric evolution was observed using an SEM. Pore parameters, including porosity (M) and abundance (C), were extracted to quantitatively analyze pore structure evolution. Particle parameters, namely probability entropy (H) and distribution fractal dimension (D), were used to quantitatively characterize particle orientation/orderliness and aggregation degree, respectively. [Results] (1) Stage-dependent recovery: Both UCS and cohesion (c) increased with thixotropic duration and showed two stages: a rapid and significant recovery phase during 0-30 d, followed by a slower, stable phase during 30-150 d. The increment during 100-150 d was small, indicating near-stabilization, after which the test was terminated. (2) Dual effect of water content: At the same thixotropic duration, UCS generally decreased with increasing water content, reflecting weakened particle contacts and bonding and thus reduced instantaneous strength. However, higher water content resulted in a faster strength recovery rate, especially at early stage, indicating that water promoted the kinetics of self-adaptive structural adjustment during thixotropic process. (3) Indicator-dependent differences: Cohesion exhibited a higher thixotropic strength ratio and faster recovery within 1 d, suggesting that shearing promoted directional particle alignment and optimized the friction-bonding interface, making c more sensitive to structural rebuilding than UCS. (4) Coordinated micro-parameter evolution: As thixotropic duration increased, M and c decreased continuously. Pores shifted from “large and numerous inter-aggregate pores” to “small and fewer intra-aggregate pores”, while the overall pore shapes remained mainly quasi-equant but became denser. Additionally, H and D decreased synchronously, indicating enhanced particle orientation/orderliness and increased aggregation. These changes were most significant within the first 30 d, consistent with the rapid macroscopic recovery stage. SEM observations revealed a transition from an “open flocculated-dispersed” fabric to a “closed flocculated-aggregated” fabric. Pores between and within aggregates decreased, while particle contacts and continuity of force-transfer paths improved, thereby supporting strength recovery. [Conclusion] The thixotropic strength recovery of Zhanjiang Formation structural clay exhibits distinct time-stage characteristics and strong sensitivity to water content. Recovery generally progresses through a rapid phase (0-30 d) and a stable phase (30-150 d). Higher water content reduces the strength level but significantly accelerates the strength recovery rate. Cohesion exhibits a higher thixotropic strength ratio than UCS because shear-induced particle orientation facilitates more effective structural reconstruction. Microscopically, synchronous decreases in M/C and H/D indicate pore reduction, particle ordering, and aggregation densification. Water enhances particle activity by altering relative particle positions and expanding migration pathways, thereby accelerating self-adaptive adjustment and strength recovery during thixotropic process. Innovations included: (1) parallel comparison of UCS and rapid direct shear parameters within a single thixotropic framework, revealing the cohesion recovery advantage caused by shear-induced particle orientation; (2) linking the macroscopic two-stage recovery pattern with the coordinated evolution of M, c, H, and D, forming an evidence chain of “structural rearrangement—aggregation densification—strength recovery”; and (3) demonstrating that higher water content, while reducing instantaneous strength, accelerates recovery by enhancing particle mobility/activity.

Key words

Zhanjiang Formation structural clay / thixotropy / strength recovery / water content

Cite this article

Download Citations
XIE Yan-hua , TANG Bin , XU Ji-cheng , et al . Influence of Water Content on Thixotropic Strength Recovery of Zhanjiang Formation Structural Clay[J]. Journal of Changjiang River Scientific Research Institute. 2026, 43(4): 166-174 https://doi.org/10.11988/ckyyb.20250292

References

[1]
臧濛, 孔令伟, 郭爱国. 静偏应力下湛江结构性黏土的动力特性[J]. 岩土力学, 2017, 38(1): 33-40.
(Zang Meng, Kong Ling-wei, Guo Ai-guo. Effects of Static Deviatoric Stress on Dynamic Characteristics of Zhanjiang Structured Clay[J]. Rock and Soil Mechanics, 2017, 38(1): 33-40. (in Chinese))
[2]
王传杰, 汤斌. 上覆压力对湛江组结构性黏土触变性的影响机制[J]. 科学技术与工程, 2023, 23(4): 1650-1657.
(Wang Chuan-jie, Tang Bin. Influence Mechanism of Overburden Pressure on Thixotropy of Structural Clay in Zhanjiang Formation[J]. Science Technology and Engineering, 2023, 23(4): 1650-1657. (in Chinese))
[3]
Seed H B, Chan C K. Thixotropic Characteristics of Compacted Clays[J]. Journal of the Soil Mechanics and Foundations Division, 1957, 83(4): 1427-1-1427-35.
[4]
刘娟娟, 曾国红, 孟令帅, 等. 扰动对粉土触变强度恢复影响规律研究[J]. 地下空间与工程学报, 2016, 12(5): 1294-1299.
Abstract
土体的触变性是导致失稳事故和工后沉降的原因之一,研究其影响因素和变化规律对于减少工程灾害具有一定的实际意义。为了探究粉土的扰动程度对其触变特性的影响,以粉土为研究对象,采用室内振动试验模拟其受扰动过程,通过无侧限抗压试验反映其强度变化,分析土体的扰动程度与其触变强度恢复程度之间的关系。结果显示:在相同频率和速率下,振动时间越长,土体受扰动程度越大;在静置时间相同的情况下,粉土的绝对强度恢复程度与其扰动程度正相关,而其相对强度恢复程度与其扰动程度负相关。建立了土体扰动程度和强度恢复程度之间的相关关系公式,为深入研究粉土工程力学性质而提供一定依据。
(Liu Juan-juan, Zeng Guo-hong, Meng Ling-shuai, et al. Study on the Effect of Disturbance on the Thixotropic Strength Increasing of Silt[J]. Chinese Journal of Underground Space and Engineering, 2016, 12(5): 1294-1299. (in Chinese))
One of the reasons for instability accidents and post-construction settlement is the thixotropy of soils, and it is meaningful for reducing engineering disasters by studying the factors and variation of soils. To explore the influence of disturbance degree of thixotropy, take the silt as research object, the laboratory vibrating model tests are carried out to simulate soil disturbance, the change of sample’s strength is reflected by unconfined compression tests. The results are used to analyze the relationship between the disturbance degree of silt and strength recovery degree. The results showed that, with the same frequence and the rate of vibrating, the disturbance degree increases with time. With the same stewing time, the absolute strength recovery degree of soil has positive correlation with the disturbance degree, while the relative strength recovery degree has negative correlation with the disturbance degree. Correlation formulas of the disturbance degree and the strength recovery degree are established, these formulas can be used to the further study of engineering properties of silt.
[5]
杨爱武, 杨少朋, 张静, 等. 天津软黏土触变特性研究[J]. 工程地质学报, 2023, 31(5): 1528-1534.
(Yang Ai-wu, Yang Shao-peng, Zhang Jing, et al. Study on Thixotropic Properties of Tianjin Soft Clay[J]. Journal of Engineering Geology, 2023, 31(5): 1528-1534. (in Chinese))
[6]
赵盛男, 霍玉龙, 汤斌. 湛江组结构性黏土触变性正交试验及其触变强度预测模型[J]. 岩土力学, 2023, 44(增刊1): 197-205.
(Zhao Sheng-nan, Huo Yu-long, Tang Bin. Thixotropic Experiment and Thixotropic Strength Prediction Model of Structural Clay in Zhanjiang Formation[J]. Rock and Soil Mechanics, 2023, 44(Supp.1): 197-205. (in Chinese))
[7]
Tang B, Zhou B, Xie L, et al. Strength Recovery Model of Clay during Thixotropy[J]. Advances in Civil Engineering, 2021, 2021: 8825107.
[8]
Shahriar A R, Jadid R. An Experimental Investigation on the Effect of Thixotropic Aging on Primary and Secondary Compression of Reconstituted Dredged Clays[J]. Applied Clay Science, 2018, 162: 524-533.
[9]
张目极. 水的存在形式对湛江组结构性黏土触变性影响的试验研究[D]. 桂林: 桂林理工大学, 2020.
(Zhang Mu-ji. Experimental Study on the Influence of Water form on the Thixotropy of Structural Clay in Zhanjiang Formation[D]. Guilin: Guilin University of Technology, 2020. (in Chinese))
[10]
霍海峰, 齐麟, 雷华阳, 等. 天津软黏土触变性的思考与试验研究[J]. 岩石力学与工程学报, 2016, 35(3):631-637.
(Huo Hai-feng, Qi Lin, Lei Hua-yang, et al. Analysis and Experimental Study on Thixotropy of Tianjin Soft Clay[J]. Chinese Journal of Rock Mechanics and Engineering, 2016, 35(3): 631-637. (in Chinese))
[11]
汤斌, 赵盛男, 周标和, 等. 基于模糊数学理论的湛江组黏土触变性强弱分级[J]. 水利水电科技进展, 2021, 41(4): 35-39, 94.
(Tang Bin, Zhao Sheng-nan, Zhou Biao-he, et al. Thixotropy Strength Classification of Zhanjiang Formation Clay Based on Fuzzy Mathematics Theory[J]. Advances in Science and Technology of Water Resources, 2021, 41(4): 35-39, 94. (in Chinese))
[12]
Alam M K, Shahriar A R, Islam M S, et al. Experimental Investigation on the Strength and Deformation Aspects of Thixotropic Aging in Reconstituted Clays[J]. Geotechnical and Geological Engineering, 2021, 39(3): 2471-2486.
[13]
张先伟, 孔令伟, 李峻, 等. 黏土触变过程中强度恢复的微观机理[J]. 岩土工程学报, 2014, 36(8): 1407-1413.
(Zhang Xian-wei, Kong Ling-wei, Li Jun, et al. Microscopic Mechanism of Strength Increase of Clay during Thixotropic Process[J]. Chinese Journal of Geotechnical Engineering, 2014, 36(8): 1407-1413. (in Chinese))
[14]
陈宝, 束庆霏, 邓荣升. 考虑板状颗粒间相互作用的黏土强度时效性的微观解释[J]. 岩土工程学报, 2021, 43(2): 271-280.
(Chen Bao, Shu Qing-fei, Deng Rong-sheng. Microscopic Interpretation of Time-dependent Strength of Clay Considering Plate-like Particle Interactions[J]. Chinese Journal of Geotechnical Engineering, 2021, 43(2): 271-280. (in Chinese))
[15]
徐永福, 王驰, 黄铭, 等. 湿喷桩施工中饱和粉土的触变性研究[J]. 岩土工程学报, 2013, 35(10):1784-1789.
(Xu Yong-fu, Wang Chi, Huang Ming, et al. Thixotropy of Saturated Silty Soils Due to Construction of DCM Columns[J]. Chinese Journal of Geotechnical Engineering, 2013, 35(10): 1784-1789. (in Chinese))
[16]
王巍. 湛江组结构性黏土触变机理研究[D]. 桂林: 桂林理工大学, 2019.
(Wang Wei. Study on Thixotropic Mechanism of Structural Clay in Zhanjiang Formation[D]. Guilin: Guilin University of Technology, 2019. (in Chinese))
[17]
肖树芳, 房后国, 王清. 软土中结合水与固结、蠕变行为[J]. 工程地质学报, 2014, 22(4): 531-535.
(Xiao Shu-fang, Fang Hou-guo, Wang Qing. The Bound Water, Consolidation and Creep Behavior of Soft Soil[J]. Journal of Engineering Geology, 2014, 22(4): 531-535. (in Chinese))
[18]
吴谦. 软粘土的结合水对其次固结和长期强度的影响及机理研究[D]. 长春: 吉林大学, 2015.
(Wu Qian. Research on Influence of Bond Water on Secondary Consolidation and Long Term Strength of Soft Clay[D]. Changchun: Jilin University, 2015. (in Chinese))
[19]
袁建滨. 粘土中结合水特性及其测试方法研究[D]. 广州: 华南理工大学, 2012.
(Yuan Jian-bin. The Study for Properties of Bound Water on Clayey Soils and Their Quantitative Methods[D]. Guangzhou: South China University of Technology, 2012. (in Chinese))
[20]
Mitchell J K. Fundamental Aspects of Thixotropy in Soils[J]. Journal of the Soil Mechanics and Foundations Division, 1960, 86(3): 19-52.
[21]
Diamond S. Pore Size Distributions in Clays[J]. Clays and Clay Minerals, 1970, 18(1): 7-23.
A knowledge of the distribution of pore sizes in clay and soil bodies is a useful element in the microstructural characterization of such materials. Pore-size distributions and total porosity of a number of reference clays, naturally-occurring subsoils, and commercial clay samples prepared in various ways were determined by mercury porosimetry. The range of equivalent pore diameter explored covered almost five orders of magnitude, from several hundred microns down to approximately 150 A. The method and its assumptions are critically evaluated, and measurements of the contact angle of mercury on clays yield values of 139° for montmorillonite and 147° for kaolinite and illite clays. The extent of shrinkage on oven-drying prior to mercury intrusion is assessed in each case and found to vary from insignificant to as much as 30 per cent of the pore space, depending on microstructural state and degree of initial saturation. The development of techniques for water removal which do not involve change in pore structure is explored. Some preliminary results for structurally weak saturated clays suggest that critical-region drying and perhaps freeze-drying procedures may be practical.
PDF(9256 KB)

Accesses

Citation

Detail

Sections
Recommended

/